致密油藏压裂井气驱暂堵调剖剂研制与评价

doi:10.3969/j.issn.1006-6535.2023.02.023

特种油气藏 ›› 2023, Vol. 30 ›› Issue (2): 161-167.DOI: 10.3969/j.issn.1006-6535.2023.02.023

致密油藏压裂井气驱暂堵调剖剂研制与评价

唐可¹, 赵勇¹, 李凯¹, 宁朦¹, 蒲万芬², 田开平²

1.中国石油新疆油田分公司,新疆克拉玛依 834000;
2.西南石油大学,四川成都 610500

收稿日期:2021-11-01 修回日期:2022-12-11 出版日期:2023-04-25 发布日期:2023-05-29
通讯作者: 田开平(1994—),男,2017年毕业于西安石油大学石油工程专业,现为西南石油大学油气田开发专业在读博士研究生,主要从事油田化学处理剂和提高采收率研究工作。
作者简介:唐可(1985—),男,工程师,2008年毕业于西南石油大学化学工程专业,2011年毕业于该校应用化学专业,获硕士学位,现从事提高采收率技术研究工作。
基金资助:
国家自然科学基金“黏度可控的原位增黏体系构建及高效驱油机理研究”(U19B2010)

Preparation and Evaluation of Temporary Plugging and Profile Control Agent for Fractured Wells in Tight Reservoirs

Tang Ke¹, Zhao Yong¹, Li Kai¹, Ning Meng¹, Pu Wanfen², Tian Kaiping²

1. PetroChina Xinjiang Oilfield Company, Karamay, Xinjiang 834000, China;
2. Southwest Petroleum University, Chengdu, Sichuan 610500, China

Received:2021-11-01 Revised:2022-12-11 Online:2023-04-25 Published:2023-05-29

摘要/Abstract

摘要： 玛湖高温致密油藏开发过程中气窜现象严重,聚合物凝胶封堵大裂缝可有效防止裂缝气窜,但同时也易封堵基质和微裂缝,造成采收率下降。为此,研制了一种耐温型暂堵调剖剂MHZD,并从成胶性能、微观形貌、注入性能、封堵能力等方面进行评价。结果表明:暂堵调剖剂配方为0.6%耐高温型阳离子聚丙烯酰胺+0.3%铬离子交联剂,该封堵体系在90 ℃高温下可以稳定成胶,成胶时间为38 h,凝胶强度为H级,凝胶稳定7~10 d后可自动降解成黏度为5.63 mPa·s的水溶液;注入暂堵剂后,岩心阻力系数小于30.000,最大突破压力梯度大于30.000 MPa/m,封堵率和解堵率均大于90%,暂堵剂可有效封堵大孔隙,动用小孔隙中的剩余油。该研究对于玛湖致密油藏压裂井封窜和提高采收率具有重要的支撑作用。

关键词: 暂堵剂, 气窜, 阻力系数, 突破压力, 致密油藏, 玛湖油田

Abstract: There is serious gas channeling in the development of Mahu high-temperature tight reservoir. Polymer gel can be used to plug large fractures, which effectively prevents gas channeling from fractures, but it also plugs matrix and micro fractures, resulting in decline in oil recovery. Therefore, a temperature-resistant temporary plugging and profile control agent MHZD was developed and evaluated from the aspects of gelling performance, microscopic morphology, injection performance and plugging capacity. The results show that: The temporary plugging and profile control agent is prepared by 0.6% temperature-resistant cationic polyacrylamide and 0.3% chromium ion cross-linking agent. The plugging system can be stably gelled at 90 ℃ within 38 h, with Grade H gel strength, and the gel can be automatically decomposed into an aqueous solution with a viscosity of 5.63 mPa·s after 7-10 d stabilization. After the injection of temporary plugging agent, the core resistance coefficient is less than 30.000, the maximum breakthrough pressure gradient is greater than 30.000 MPa/m, and the plugging rate and unplugging rate are both greater than 90%. The temporary plugging agent can effectively plug the large pores and recover the remaining oil in the small pores. This study plays an underlying role in plugging against gas channeling and enhancing oil recovery of fractured wells in Mahu tight reservoir.

Key words: temporary plugging agent, gas channeling, resistance coefficient, breakthrough pressure, tight reservoir, Mahu Oilfield

中图分类号:

TE355

唐可, 赵勇, 李凯, 宁朦, 蒲万芬, 田开平. 致密油藏压裂井气驱暂堵调剖剂研制与评价[J]. 特种油气藏, 2023, 30(2): 161-167.

Tang Ke, Zhao Yong, Li Kai, Ning Meng, Pu Wanfen, Tian Kaiping. Preparation and Evaluation of Temporary Plugging and Profile Control Agent for Fractured Wells in Tight Reservoirs[J]. Special Oil & Gas Reservoirs, 2023, 30(2): 161-167.

参考文献

[1] 罗天雨,芳桂,梁丽娟,等.化学暂堵剂在石油工程方面的研究新进展及应用[J].新疆石油天然气,2019,15(3):79-87.
LUO Tianyu,FANG Gui,LIANG Lijuan,et al.New progress and application of chemical temporary plugging agents in petroleum engineering[J].Xinjiang Oil & Gas,2019,15(3):79-87.
[2] 姜相.化学暂堵剂在石油工程方面的研究与应用[J].科学技术创新,2019,23(34):57-58.
JIANG Xiang.Research and application of chemical temporary plugging agents in petroleum engineering[J].Scientific and Technological Innovation,2019,23(34):57-58.
[3] ZHAO Guang,DAI Caili,LI Weitao,et al.Research on a temporary plugging agent based on polymer gel for reservoir acidification[J].Journal of Petroleum Exploration & Production Technology,2016,6(3):465-472.
[4] ALMUNTASHERI G A,NASRELDIN H A,ZITHA P L,et al.Gelation kinetics and performance evaluation of an organically crosslinked gel at high temperature and pressure[J].SPE Journal,2008,13(3):337-345.
[5] KUMAR A,MAHTO V,CHOUBEY A K,et al.Synthesis and characterization of cross-linked hydrogels using polyvinyl alcohol and polyvinyl pyrrolidone and their blend for water shut-off treatments[J].Journal of Molecular Liquids,2020,301:112472.
[6] 张家旗,黄维安,程荣超,等.淀粉基可降解暂堵剂制备及性能评价[J].应用化工,2021,50(9):1-6.
ZHANG Jiaqi,HUANG Weian,CHENG Rongchao,et al.Development and evaluation of starch-based biodegradable temporary plugging agent[J].Applied Chemical Industry,2021,50(9):1-6.
[7] 许江文,张谷畅,李建民,等.暂堵剂形状对裂缝封堵影响规律的实验研究[J].断块油气田,2022,29(6):842-847.
XU Jiangwen,ZHANG Guchang,LI Jianmin,et al.Experimental study on influence law of temporary plugging agent shape on fracture plugging[J].Fault-Block Oil & Gas Field,2022,29(6):842-847.
[8] 李建辉,李想,岳明,等.长庆油田宽带压裂储层产能模型及渗流规律研究[J].石油钻探技术,2022,50(6):112-119.
LI Jianhui,LI Xiang,YUE Ming,et al.Productivity model and seepage rules for the broadband fracturing of ultra-low permeability reservoirs in Changqing Oilfield[J].Petroleum Drilling Techniques,2022,50(6):112-119.
[9] 孟丽艳,张麒麟,张希红,等.钻井液用聚合物暂堵剂室内研究与评价[J].精细石油化工进展,2012,13(5):1-6.
MENG Liyan,ZHANG Qilin,ZHANG Xihong,et al.Research and evaluation of polymer temporary plugging agent for drilling fluid[J].Advances in Fine Petrochemicals,2012,13(5):1-6.
[10] 杨恒林,吕嘉昕,谭鹏,等.基于三维扫描技术的页岩暂堵压裂物理模拟实验[J].断块油气田,2022,29(1):118-123.
YANG Henglin,LYU Jiaxin,TAN Peng,et al.Physical simulation experiment on shale temporary plugging and fracturing based on 3D scanning technology[J].Fault-Block Oil & Gas Field,2022,29(1):118-123.
[11] 李玉娇,吕开河.自适应广谱屏蔽暂堵剂ZPJ研究[J].钻采工艺,2007,20(3):111-112.
LI Yujiao,LYU Kaihe.Study on autoadapted shielding temporary plugging agent ZPJ[J].Drilling & Production Technology,2007,20(3):111-112.
[12] 吴峙颖,胡亚斐,蒋廷学,等.孔洞型碳酸盐岩储层压裂裂缝转向扩展特征研究[J].石油钻探技术,2022,50(4):90-96.
WU Zhiying,HU Yafei,JIANG Tingxue,et al.Study on propagation and diversion characteristics of hydraulic fractures in vuggy carbonate reservoirs[J].Petroleum Drilling Techniques,2022,50(4):90-96.
[13] 姜歆,王博通,樊英,等.油溶性树脂暂堵剂的室内评价[J].科学技术与工程,2010,10(31):7721-7723.
JIANG Xin,WANG Botong,FAN Ying,et al.The interior estimation of oil soluble resin temporary plugging additive[J].Science Technology and Engineering,2010,10(31):7721-7723.
[14] 达引朋,李建辉,王飞,等.长庆油田特低渗透油藏中高含水井调堵压裂技术[J].石油钻探技术,2022,50(3):74-79.
DA Yinpeng,LI Jianhui,WANG Fei,et al.Fracturing technologies with profile control and water shutoff for medium and high water-cut wells in ultra-low permeability reservoirs of Changqing Oilfield[J].Petroleum Drilling Techniques,2022,50(3):74-79.
[15] 张易航,陈瞰瞰,石锋.高强度暂堵剂的制备及破胶性能研究[J].当代化工,2016,45(6):1101-1103.
ZHANG Yihang,CHEN Kankan,SHI Feng.Preparation of high strength of temporary plugging agent and its gel breaking performance[J].Contemporary Chemical Industry,2016,45(6):1101-1103.
[16] 张艳英,蒲万芬,唐山,等.低温油藏深部调驱用弱凝胶体系研究[J].应用化工,2012,41(4):570-572.
ZHANG Yanying,PU Wanfen,TANG Shan,et al.Research of weak gel system for in-depth profile control in low temperature reservoirs[J].Applied Chemical Industry,2012,41(4):570-572.
[17] 杨子浩,罗智忆,林梅钦,等.改善低渗油藏二氧化碳气驱油效果的耐温泡沫凝胶体系的构建[J].油田化学,2020,37(1):86-92.
YANG Zihao,LUO Zhiyi,LIN Meiqin,et al.Preparation of temperature resistant foam gel system for improving CO₂ gas flooding effect in low permeability reservoir[J].Oilfield Chemistry,2020,37(1):86-92.
[18] 赵冀,蒲万芬,李科星,等.一种大孔道超强堵剂的室内实验研究[J].钻采工艺,2008,31(5):133-136.
ZHAO Ji,PU Wanfen,LI Kexing,et al.Experimental study on a super strong macropore blocking agent[J].Drilling & Production Technology,2008,31(5):133-136.
[19] 李娟,邓红英,张丽.氨基酸螯合亚铁的室温固相合成及表征[J].绵阳师范学院学报,2017,36(8):72-76.
LI Juan,DENG Hongying,ZHANG Li.Solid-state synthesis and characterization of ferrous amino acid chelate at room temperature[J].Journal of Mianyang Normal University,2017,36(8):72-76.
[20] 王晓惠,赵玲莉,孔明炜,等.暂堵凝胶在水平井堵水中的应用[J].石油天然气学报,2010,32(2):352-354.
WANG Xiaohui,ZHAO Lingli,KONG Mingwei,et al.Application of temporary-blocking agent for water plugging in horizontal wells[J].Journal of Oil and Gas Technology,2010,32(2):352-354.
[21] 张涵,李笃.调剖剂室内配方研究[J].内江科技,2013,34(10):108-166.
ZHANG Han,LI Du.Study on the indoor formulation of profile control agent[J].Neijiang Science & Technology,2013,34(10):108-166.
[22] 李业.泡沫油制备及阻力特性研究[D].成都:西南石油大学,2014.
LI Ye.Research on the preparation and resistance characteristics of foam oil[D].Chengdu:Southwest Petroleum University,2014.
[23] 张文涛.毛细管突破压力模拟实验及页岩封闭能力[J].石油实验地质,2018,40(4):577-582.
ZHANG Wentao.Experimental study of the breakthrough pressure of capillaries and the sealing ability of shale[J].Petroleum Geology & Experiment,2018,40(4):577-582.
[24] 曹坤.堵水调剖方法及封堵效果评价研究[D].东营:中国石油大学(华东),2010.
CAO Kun.Research on the water plugging and profile control method and evaluation of plugging effect[D].Dongying:China University of Petroleum(East China),2010.
[25] 李泽锋,高燕,王祖文,等.油溶性暂堵剂YDJ-1的制备及性能评价[J].油田化学,2021,38(1):47-51.
LI Zefeng,GAO Yan,WANG Zuwen,et al.Preparation and performance evaluation of oil-soluble plugging agent YDJ-1[J].Oilfield Chemistry,2021,38(1):47-51.

致密油藏压裂井气驱暂堵调剖剂研制与评价

Preparation and Evaluation of Temporary Plugging and Profile Control Agent for Fractured Wells in Tight Reservoirs

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